N,N-二甲基-2-苯乙胺合成路线 （共 89 条）
反应条件
1: KF / dimethylformamide / 145 - 150 °C 2: aq. NaOH 3: (i) SOCl2, (ii) /BRN= 605257/ 4: LiAlH4 View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 528 - 530
反应条件
titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 10 h, 2.) 25 deg C, 10 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 60, # 15 p. 4928 - 4929
反应条件
1: alcohol; ammonium hydrosulfide / 70 °C 2: amalgamated aluminium; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 431, p. 213
Chem. Zentralbl., , vol. 94, # II p. 403
反应条件
4-methyl-morpholine; lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; Wang resin 1.) 0 deg C, 2 h; room temp., overnight, 2.) DMF, room temp., overnight, 3.) THF, 60 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 38, # 16 p. 2799 - 2802
反应条件
lithium aluminium tetrahydride
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 528 - 530
参考文献
Chemische Berichte, , vol. 45, p. 2404
Justus Liebigs Annalen der Chemie, , vol. 395, p. 344
反应条件
1: 170 - 180 °C / weiteres Edukt: Schwefel; im Rohr 2: sulfuric acid / 30 - 40 °C / Electrolysis.an Bleikathoden View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 431, p. 213
Chem. Zentralbl., , vol. 94, # II p. 403
反应条件
1: potassium sulfide; xylene; phosphorus pentasulfide / 70 - 80 °C 2: amalgamated aluminium; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 431, p. 213
Chem. Zentralbl., , vol. 94, # II p. 403
反应条件
1: 170 - 180 °C / weiteres Edukt: Schwefel; im Rohr 2: sulfuric acid / 30 - 40 °C / Electrolysis.an Bleikathoden View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 431, p. 213
Chem. Zentralbl., , vol. 94, # II p. 403
反应条件
1: (i) SOCl2, (ii) /BRN= 605257/ 2: LiAlH4 View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 528 - 530
