1: 93 percent / LiAlH4 / diethyl ether / 1 h / -40 °C 2: MnO2 / petroleum ether; diethyl ether / 168 h / Ambient temperature 3: pyridinium p-toluenesulfonate / ethanol / 12 h / 55 °C View Scheme
参考文献
Tsuboi, Sadao; Mimura, Shigetoshi; Ono, Shin-ichiro; Watanabe, Kenji; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1807 - 1812
With lithium aluminium tetrahydride in diethyl ether T=-40°C; 1 h;
参考文献
Tsuboi, Sadao; Mimura, Shigetoshi; Ono, Shin-ichiro; Watanabe, Kenji; Takeda, Akira Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1807 - 1812
Multi-step reaction with 2 steps 1: 93 percent / LiAlH4 / diethyl ether / 1 h / -40 °C2: MnO2 / petroleum ether; diethyl ether / 168 h / Ambient temperature
参考文献
Tsuboi, Sadao; Mimura, Shigetoshi; Ono, Shin-ichiro; Watanabe, Kenji; Takeda, Akira Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1807 - 1812
