D-N-Boc-3-甲基吗啉合成路线 (共 6 条)
反应条件
N-bromosuccinmide in tetrachloromethane 1 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 113, # 23 p. 8796 - 8806
反应条件
1: NaHCO3, NaCl / CHCl3; H2O / 20 h / Heating 2: 73.4 percent / p-toluenesulfonic acid monohydrate, CaCl2 / benzene / 8 h / Heating 3: N-bromosuccinimide / CCl4 / 1 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, # 5 p. 1547 - 1557
反应条件
1: 84.3 percent / triethylamine / tetrahydrofuran / 18 h 2: NaHCO3, NaCl / CHCl3; H2O / 20 h / Heating 3: 73.4 percent / p-toluenesulfonic acid monohydrate, CaCl2 / benzene / 8 h / Heating 4: N-bromosuccinimide / CCl4 / 1 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, # 5 p. 1547 - 1557
反应条件
1: NaHCO3, NaCl / CHCl3; H2O / 20 h / Heating 2: 73.4 percent / p-toluenesulfonic acid monohydrate, CaCl2 / benzene / 8 h / Heating 3: N-bromosuccinimide / CCl4 / 1 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, # 5 p. 1547 - 1557
反应条件
1: 73.4 percent / p-toluenesulfonic acid monohydrate, CaCl2 / benzene / 8 h / Heating 2: N-bromosuccinimide / CCl4 / 1 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 110, # 5 p. 1547 - 1557
反应条件
1: 63 percent / ZnCl2 / tetrahydrofuran / 4 h 2: 71 percent / Li, NH3 / ethanol; tetrahydrofuran / 0.25 h / -33 °C View Scheme
参考文献
Williams, Robert M.; Sinclair, Peter J.; Zhai, Dongguan; Chen, Daimo
Journal of the American Chemical Society, 1988 , vol. 110, # 5 p. 1547 - 1557