1-(2-溴-5-羟基苯基)乙酮合成路线 (共 4 条)
反应条件
[BBIm]Br3
T=20°C; 0.166667 h; Neat (no solvent); regioselective reaction;
参考文献
Borikar; Daniel
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 2 p. 531 - 536
反应条件
1: With toluene-4-sulfonic acid in water; acetonitrile
T=20°C; 0.0333333 h;
2: With N-bromosuccinmide in water; acetonitrile
T=20°C; 2 h; regioselective reaction;
参考文献
Bovonsombat, Pakorn; Ali, Rameez; Khan, Chiraphorn; Leykajarakul, Juthamard; Pla-On, Kawin; Aphimanchindakul, Suraj; Pungcharoenpong, Natchapon; Timsuea, Nisit; Arunrat, Anchalee; Punpongjareorn, Napat
Tetrahedron, 2010 , vol. 66, # 34 p. 6928 - 6935
反应条件
N-bromosuccinmide in acetonitrile
T=20°C; 2 h; regioselective reaction;
参考文献
Bovonsombat, Pakorn; Ali, Rameez; Khan, Chiraphorn; Leykajarakul, Juthamard; Pla-On, Kawin; Aphimanchindakul, Suraj; Pungcharoenpong, Natchapon; Timsuea, Nisit; Arunrat, Anchalee; Punpongjareorn, Napat
Tetrahedron, 2010 , vol. 66, # 34 p. 6928 - 6935
反应条件
1: With N-bromosuccinmide in water; acetonitrile
T=20°C; 0.25 h;
2: With toluene-4-sulfonic acid in vaseline; acetonitrile
T=20°C; 2 h; regioselective reaction;
参考文献
Bovonsombat, Pakorn; Ali, Rameez; Khan, Chiraphorn; Leykajarakul, Juthamard; Pla-On, Kawin; Aphimanchindakul, Suraj; Pungcharoenpong, Natchapon; Timsuea, Nisit; Arunrat, Anchalee; Punpongjareorn, Napat
Tetrahedron, 2010 , vol. 66, # 34 p. 6928 - 6935