4-(1,1-二甲基乙基)-3,5-环己二烯-1,2-二酮合成路线 (共 24 条)
反应条件
hydrogen; potassium carbonate; palladium on activated charcoal in N,N-dimethyl-formamide
P=760.051 Torr; 12 h;
参考文献
Magdziak, Derek; Rodriguez, Andy A.; Van De Water, Ryan W.; Pettus, Thomas R. R.
Organic Letters, 2002 , vol. 4, # 2 p. 285 - 288
反应条件
1: 45 percent / 1 h / Ambient temperature; Irradiation
2: potassium carbonate / ethane-1,2-diol / 4 h / 120 °C
View Scheme
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
sodium hydroxide; sodium metasilicate; diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; dihydrogen peroxide in water
T=40°C; 1 h; pH 10.0; Mechanism;
参考文献
Gellerstedt, Goeran; Hardell, Hanne-Lise; Lindfors, Eva-Lisa
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 9 p. 669 - 674
反应条件
1: With [bis(2-methoxyethyl)amino]-sulfur trifluoride in chloroform
T=0 - 20°C; Inert atmosphere;
2: With sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene in ethanol
T=0 - 50°C;
参考文献
Nemoto, Hiroyuki; Nishiyama, Tsuyoshi; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 10 p. 2714 - 2717