in melt MoO3, SiO2, Mg and NaCl mixed for 12 h, pressed, combusted at 1300, 1520, 1800°C with ignition agent Ti+C; treated with HCl and NaOH; monitored by XRD;
参考文献
Nersisyan, Hayk H.; Won, Hyung Il; Won, Chang Whan
Journal of the American Ceramic Society, 2008 , vol. 91, # 9 p. 2802 - 2807
in solid Kinetics; byproducts: SiO2, 2FeO*SiO2, FeO; in graphite or alumina furnace at 900-1000°C at pressure of 2.6E-4 Pa for 30-240 min; elem. anal., metallographic and scanning electron microscopy;
参考文献
Tomsia; Pask
Journal of the American Ceramic Society, 1981 , vol. 64, # 9 p. 523 - 528
in neat (no solvent) slight excess over the stoich. amt. of COF2 required; reaction mixt. heated in a stainless steel or monel cylinder at 160°C for 36 h;