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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
112930-69-5
合成路线
（共 5 条）
112930-66-2
→
反应条件
112930-69-5
反应条件
ammonia in chloroform 1) 10 deg C, 1 h; 2) room temp., 3 h;
参考文献
Polivka, Zdenek; Licha, Irena; Taufmann, Petr; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1566 - 1581
1531-77-7
6,11-二氢二苯并[b,e]硫杂卓-11-酮
→
反应条件
112930-69-5
反应条件
1: 1) Mg / in THF 2: 94 percent / HBr / acetic acid / 1 h / 15 °C 3: 80 percent / tetrahydrofuran; ethanol; H2O / 1.5 h / Ambient temperature 4: aq. KOH / ethanol / 3.5 h / Heating 5: 97 percent / SOCl2 / benzene / 3 h / Heating 6: 64 percent / NH3 / CHCl3 / 1) 10 deg C, 1 h; 2) room temp., 3 h View Scheme
参考文献
Polivka, Zdenek; Licha, Irena; Taufmann, Petr; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1566 - 1581
112930-52-6
→
反应条件
112930-69-5
反应条件
1: 94 percent / HBr / acetic acid / 1 h / 15 °C 2: 80 percent / tetrahydrofuran; ethanol; H2O / 1.5 h / Ambient temperature 3: aq. KOH / ethanol / 3.5 h / Heating 4: 97 percent / SOCl2 / benzene / 3 h / Heating 5: 64 percent / NH3 / CHCl3 / 1) 10 deg C, 1 h; 2) room temp., 3 h View Scheme
参考文献
Polivka, Zdenek; Licha, Irena; Taufmann, Petr; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1566 - 1581
112930-58-2
(3E)-3-(6H-苯并[c][1]苯并硫杂卓-11-亚基)丙酸
→
反应条件
112930-69-5
反应条件
1: 97 percent / SOCl2 / benzene / 3 h / Heating 2: 64 percent / NH3 / CHCl3 / 1) 10 deg C, 1 h; 2) room temp., 3 h View Scheme
参考文献
Polivka, Zdenek; Licha, Irena; Taufmann, Petr; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1566 - 1581
112930-54-8
→
反应条件
112930-69-5
反应条件
1: 80 percent / tetrahydrofuran; ethanol; H2O / 1.5 h / Ambient temperature 2: aq. KOH / ethanol / 3.5 h / Heating 3: 97 percent / SOCl2 / benzene / 3 h / Heating 4: 64 percent / NH3 / CHCl3 / 1) 10 deg C, 1 h; 2) room temp., 3 h View Scheme
参考文献
Polivka, Zdenek; Licha, Irena; Taufmann, Petr; Svatek, Emil; Holubek, Jiri; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 6 p. 1566 - 1581
