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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
112933-58-1
合成路线
（共 9 条）
7190-52-5
→
反应条件
112933-58-1
反应条件
trichlorophosphate in toluene T=70°C;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
20730-02-3
N-苯基丙肼
→
反应条件
112933-58-1
反应条件
1: 65 percent / NaOEt / ethanol / 5 h / Heating 2: 75 percent / conc. HCl / 1 h / Heating 3: 61 percent / phosphorous oxychloride / toluene / 1 h / 80 °C View Scheme
参考文献
Dowlatshahi, Hossein A.
Synthetic Communications, 1987 , vol. 17, # 10 p. 1253 - 1260
1765-93-1
4-氟苯硼酸
+
112933-58-1
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
+
75343-38-3
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
32316-92-0
2-萘硼酸
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
128796-39-4
4-三氟甲基苯硼酸
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
139301-27-2
4-三氟甲氧基苯硼酸
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
98-80-6
苯硼酸
→
反应条件
73747-25-8
4-(苯基氨基)丁腈
+
24398-61-6
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
55552-70-0
+
112933-58-1
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
112933-58-1
+
182163-96-8
3,4,5-三甲氧基苯硼酸
→
反应条件
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
