4-苯基吡啶-N-氧化物合成路线 (共 20 条)
反应条件
diethylamine in ethyl acetate T=17°C; Irradiation;
参考文献
Heterocycles, , vol. 27, # 1 p. 113 - 124
反应条件
diethylamine in ethanol T=17°C; Irradiation;
参考文献
Heterocycles, , vol. 27, # 1 p. 113 - 124
反应条件
in ethanol T=17°C; Irradiation;
参考文献
Heterocycles, , vol. 27, # 1 p. 113 - 124
反应条件
N,N-dimethylcarbamoyl chloride in 1-nitroethane T=20°C; 45 h;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP1424336 A1, 2004 ;
Location in patent: Page 104 ;
反应条件
potassium carbonate in dichloromethane
参考文献
Merck and Co., Inc.
Patent: US5494919 A1, 1996 ;
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4555520 A1, 1985 ;
反应条件
1: in tetrahydrofuran T=25°C; 2: With acetic anhydride T=120°C; 0.0666667 h; microwave irradiation; Further stages.;
参考文献
Andersson, Hans; Almqvist, Fredrik; Olsson, Roger
Organic Letters, 2007 , vol. 9, # 7 p. 1335 - 1337
反应条件
copper acetylacetonate; potassium tert-butylate; oxygen in toluene T=110°C; 2 h;
参考文献
Shen, Yan; Chen, Jiuxi; Liu, Miaochang; Ding, Jinchang; Gao, Wenxia; Huang, Xiaobo; Wu, Huayue
Chemical Communications, 2014 , vol. 50, # 33 p. 4292 - 4295
反应条件
diethyl ether; benzene
参考文献
Colonna; Risaliti
Annali di Chimica (Rome, Italy), 1958 , vol. 48, p. 1395,1396
反应条件
in tetrahydrofuran
T=0 - 25°C; Methylation; Deoxygenation; 2 h;
参考文献
Nicolaou; Koumbis, Alexandros E.; Snyder, Scott A.; Simonsen, Klaus B.
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 14 p. X2529-2533