3,4-二甲氧基苯乙酮合成路线 （共 188 条）
反应条件
1: With ammonium acetate; acetic acid in toluene
Gewald Aminoheterocycles Synthesis; Dean-StarkReflux;
2: With sulfur; diethylamine in ethanol
T=50°C; Gewald Aminoheterocycles Synthesis; 3 h;
参考文献
Titchenell, Paul M.; Hollis Showalter; Pons, Jean-Francois; Barber, Alistair J.; Jin, Yafei; Antonetti, David A.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 10 p. 3034 - 3038
反应条件
1,4-diaza-bicyclo[2.2.2]octane; hydroxylamine hydrochloride
0.0666667 h; Microwave irradiationIonic liquid;
参考文献
Hajipour; Rafiee; Ruoho
Journal of the Iranian Chemical Society, 2010 , vol. 7, # 1 p. 114 - 118
参考文献
Jugelt, Werner; Schwertner, Siegfried
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 11 p. 409 - 410
参考文献
Jugelt, Werner; Schwertner, Siegfried
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 11 p. 409 - 410
反应条件
1: 8 percent / KOH (s) / dimethylsulfoxide / Ambient temperature
2: 49 percent / Raney-nickel W2 / ethanol / 10 h / Heating
View Scheme
参考文献
Tominaga, Yoshinori; Ushirogochi, Atsuyuki; Matsuda, Yoshiro
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1557 - 1567
反应条件
1: 5.5 g / sodium hydride / tetrahydrofuran / 48 h / Ambient temperature
2: 515 mg / lithium aluminium hydride / tetrahydrofuran / 0.5 h / 0 °C / stirring at r.t. for 2 hrs.,
View Scheme
参考文献
Biftu, Tesfaye
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 881 - 884
反应条件
1: pyridinium hydrobromide perbromide / chloroform; ethanol / 16 h / 50 °C
2: sodium azide / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere
3: aluminum oxide; sodium tetrahydroborate / diethyl ether / 16 h / 20 °C / Inert atmosphere
4: hydrogen / palladium 10 on activated carbon / methanol
View Scheme
参考文献
UCL BUSINESS PLC; BIRKBECK COLLEGE; WAKSMAN, Gabriel; TABOR, Alethea; SAYER, James; WALLDEN, Karin
Patent: WO2012/168733 A1, 2012 ;
WO 2012/168733 A1
反应条件
selenium(IV) oxide in pyridine
4.5 h; Heating;
参考文献
Pirrung, Michael C.; Tepper, Ronald J.
Journal of Organic Chemistry, 1995 , vol. 60, # 8 p. 2461 - 2465
参考文献
Neitzel
Chemische Berichte, 1891 , vol. 24, p. 2867
反应条件
FibreCatTM 1000-D7; sodium t-butanolate in tetrahydrofuran
T=85°C; 6 h;
参考文献
Churruca, Fatima; SanMartin, Raul; Carril, Monica; Tellitu, Imanol; Dominguez, Esther
Tetrahedron, 2004 , vol. 60, # 10 p. 2393 - 2408
