3,4-二甲氧基苯乙酮合成路线 （共 188 条）
反应条件
1-benzyl-1-aza-4-azoniabicyclolt;2.2.2gt;octane periodate in acetonitrile Oxidation; 0.25 h; Heating;
参考文献
Hajipour, Abdol Reza; Mohammadpoor-Baltork, Iraj; Niknam, Kurosh
Organic Preparations and Procedures International, 1999 , vol. 31, # 3 p. 335 - 341
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Mahendar, Lodi; Satyanarayana, Gedu
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2059 - 2074
反应条件
1: With N-iodo-succinimide; N-hexadecyl-N,N,N-trimethylammonium bromide in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation; 2: With dipyridinium dichromate; acetic acid in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Naina; Sharma, Abhishek; Kumar, Rakesh; Shard, Amit; Sinha, Arun K.
European Journal of Organic Chemistry, 2010 , # 31 p. 6025 - 6032
反应条件
silver perchlorate; niobium pentachloride in nitromethane T=80°C; Friedel-Crafts acylation; 3 h;
参考文献
Arai, Shigeru; Sudo, Yukinori; Nishida, Atsushi
Tetrahedron, 2005 , vol. 61, # 19 p. 4639 - 4642
反应条件
ruthenium(II)-carbonyl-tris(triphenylphosphine) dihydride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=135°C; 4 h; Inert atmosphere;
参考文献
Nichols, Jason M.; Bishop, Lee M.; Bergman, Robert G.; Ellman, Jonathan A.
Journal of the American Chemical Society, 2010 , vol. 132, # 36 p. 12554 - 12555
反应条件
1: in tetrahydrofuran T=0°C; 0.5 h; Green chemistry; 2: With [bis(acetoxy)iodo]benzene T=0 - 20°C; 1 h; Green chemistry; Reagent/catalystTime;
参考文献
Sagara, Prateep Singh; Chebolu, Rajesh; Bahuguna, Ashish; Ravikumar
RSC Advances, 2014 , vol. 4, # 29 p. 15011 - 15013
反应条件
5 palladium on charcoal; ammonium formate in tert-butyl methyl ether; water T=80°C; 3 h;
参考文献
Galkin, Maxim V.; Sawadjoon, Supaporn; Rohde, Volker; Dawange, Monali; Samec, Joseph S. M.
ChemCatChem, 2014 , vol. 6, # 1 p. 179 - 184
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; potassium 2-methyl-2-butoxide; ethyl acetate in toluene T=140°C; 18 h; Schlenk techniqueSealed tubeInert atmosphere; chemoselective reaction;
参考文献
ChemCatChem, , vol. 5, # 8 p. 2170 - 2173
反应条件
in tetrahydrofuran T=-10°C;
参考文献
Kumar, Amit; Akula, Hari Kiran; Lakshman, Mahesh K.
European Journal of Organic Chemistry, 2010 , # 14 p. 2709 - 2715
反应条件
potassium carbonate in acetone 0.75 h; Heating;
参考文献
Khatib, Soliman; Nerya, Ohad; Musa, Ramadan; Shmuel, Maayan; Tamir, Snait; Vaya, Jacob
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 2 p. 433 - 441
