3,4-二甲氧基苯乙酮合成路线 (共 188 条)
反应条件
Candida antarctica lipase B immobilized; dihydrogen peroxide in water T=60°C; 8 h; Ionic liquidEnzymatic reaction; chemoselective reaction;
参考文献
Sharma, Upendra K.; Sharma, Nandini; Kumar, Rakesh; Kumar, Rajesh; Sinha, Arun K.
Organic Letters, 2009 , vol. 11, # 21 p. 4846 - 4848
反应条件
toluene-4-sulfonic acid in water 7 h; Heating;
参考文献
Synthetic Communications, , vol. 37, # 10 p. 1665 - 1673
反应条件
Ph2BSbCl6 in dichloromethane 24 h; Ambient temperature;
参考文献
Mukaiyama, Teruaki; Nagaoka, Hitoshi; Ohshima, Masahiro; Murakami, Masahiro
Chemistry Letters, 1986 , p. 165 - 168
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Heterocycles, , vol. 44, # 1 p. 139 - 142
反应条件
dichloro bis(acetonitrile) palladium(II); water; oxygen; copper dichloride in toluene; tert-butyl alcohol T=60°C; Wacker Oxidation; P=6000.6 Torr; 1 h; Flow reactor;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 10 p. 1905 - 1910
反应条件
copper T=230 - 240°C; 0.25 h;
参考文献
Sanceau, Jean-Yves; Dhal, Robert; Brown, Eric
Tetrahedron, 1994 , vol. 50, # 11 p. 3363 - 3380
反应条件
(1R,2S,9S)-11-methyl-13-oxa-7,11-diazatricyclo[7.3.1.02,7]tridecane; C11H20Br2N2OPd; oxygen; caesium carbonate in chloroform T=20°C; 21.6 h; Molecular sieve; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 74, # 3 p. 1407 - 1410
反应条件
Nocardia corallina B-276 in octane; N,N-dimethyl-formamide T=28 - 30°C; 25 h; Enzymatic reaction;
参考文献
Tetrahedron Asymmetry, , vol. 12, # 12 p. 1709 - 1712
反应条件
trifluoroacetic acid T=120°C; Nazarov cyclization; 0.333333 h; microwave irradiation;
参考文献
Lawrence, Nicholas J.; Armitage, E. Simon M.; Greedy, Benjamin; Cook, Darren; Ducki, Sylvie; McGown, Alan T.
Tetrahedron Letters, 2006 , vol. 47, # 10 p. 1637 - 1640
反应条件
disodium octaborate; dipotassium peroxodisulfate; tert-butyl alcohol T=20°C; pH=10; Radiolysis;
参考文献
Chemistry - A European Journal, , vol. 7, # 7 p. 1408 - 1416