3,4-二甲氧基苯乙酮合成路线 （共 188 条）
反应条件
1: tetrahydrofuran 2: aq. K2S2O8; 2-methyl-2-propanol; disodium tetraborate decahydrate / 20 °C / pH 10 / Radiolysis View Scheme
参考文献
Chemistry - A European Journal, , vol. 7, # 7 p. 1408 - 1416
参考文献
Journal of the American Pharmaceutical Association (1912-1977), , vol. 45, p. 440
反应条件
hydrogenchloride in methanol 2 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 22, p. 1323 - 1324
反应条件
1: 100 percent / diethyl ether; tetrahydrofuran / 1 h / Heating 2: 65 percent / Jones reagent / acetone / 4 °C 3: Cu powder / 0.25 h / 230 - 240 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 11 p. 3363 - 3380
反应条件
in isopropyl alcohol 15 h; IrradiationInert atmosphere;
参考文献
Tazhe Veetil, Aneesh; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Pavlikova, Nela; Heger, Dominik; Klan, Petr
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8232 - 8242
反应条件
sodium perchlorate; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3582,3585
反应条件
1.1: 99 percent / thionyl chloride; urea / toluene / 3 h / 100 °C 2.1: magnesium; ethanol / toluene; CCl4 / 1 h / Heating 2.2: 95 percent / toluene; CCl4 / 0.5 h / 20 °C 3.1: 5 percent / p-TsOH*H2O / H2O / 7 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 37, # 10 p. 1665 - 1673
反应条件
1: 1.) n-BuLi, N-isopropylcyclohexylamine / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, -78 deg C, 15 min 2: 4.5 h / Mortierella isabelina View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 7, # 4 p. 1077 - 1088
反应条件
potassium carbonate; xylene T=130°C;
参考文献
Journal of the Chemical Society, , vol. 105, p. 1051
反应条件
oxygen; sodium hydrogencarbonate; methyl viologen triflate in water 1 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 70, # 7 p. 2720 - 2728
