5,6,7,8-四羟基-2-萘甲酸合成路线 (共 39 条)
反应条件
1: With sodium hydroxide; water in tetrahydrofuran T=60°C; 20 h; 2: With hydrogenchloride in water pH=3 - 5;
参考文献
WO2008/95058 A1, ;
Page/Page column 37-38 ;
反应条件
sodium hydroxide in tetrahydrofuran T=60°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 49, # 21 p. 4033 - 4044
反应条件
1,4-dioxane; sodium hydroxide; nickel T=150°C; P=175051 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 576,578
反应条件
sodium hypobromide in water 1.) 3 h, 0 deg C; 2.) 2.5 h, room temp.;
参考文献
Monatshefte fuer Chemie, , vol. 120, p. 597 - 622
反应条件
1: With n-butyllithium in Dry THF; hexane T=-78 - 25°C; 1.16667 h; 2: With hydrogenchloride pH=1;
参考文献
WO2004/792 A1, ;
Page 22 ;
反应条件
sodium hydroxide; nickel; sodium carbonate T=100°C; P=128714 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 73, p. 1393,1397
反应条件
sodium hydroxide; ethanol; platinum T=100°C; P=128714 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 73, p. 1393,1397
反应条件
1: AlCl3; CS2 2: KMnO4; acetone View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 3747
反应条件
permanganate(VII) ion
参考文献
Chemische Berichte, , vol. 55, p. 1708
反应条件
sodium hydroxide; hydrogen; platinum(IV) oxide in ethanol T=30°C; Title compound not separated from byproducts;
参考文献
Biodegradation, , vol. 11, # 2-3 p. 117 - 124