苄基4-(溴甲基)苯甲酸酯合成路线 （共 8 条）
反应条件
toluene-4-sulfonic acid in toluene Esterification; 18 h; Heating;
参考文献
Henley, Peter D.; Waymark, Christopher P.; Gillies, Iain; Kilburn, Jeremy D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 6 p. 1021 - 1031
反应条件
sodium hydrogencarbonate T=20°C; Esterification; 5 h;
参考文献
Konya, Klara G.; Paul, Thomas; Lin, Shuqiong; Lusztyk, Janusz; Ingold
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7518 - 7527
反应条件
4-(N,N-dimethlyamino)pyridine; benzyl alcohol in tetrahydrofuran
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4711900 A1, 1987 ;
反应条件
1: 93 percent / SOCl2 / 3 h / Heating 2: 86 percent / NaHCO3 / 5 h / 20 °C View Scheme
参考文献
Konya, Klara G.; Paul, Thomas; Lin, Shuqiong; Lusztyk, Janusz; Ingold
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7518 - 7527
反应条件
1: DCCI, DMAP / CH2Cl2 / Ambient temperature 2: NaBH4 3: PBr3 View Scheme
参考文献
Scherowsky, G.; Sefkow, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 202, p. 207 - 216
反应条件
1: DCCI, DMAP / CH2Cl2 / Ambient temperature 2: NaBH4 3: PBr3 View Scheme
参考文献
Scherowsky, G.; Sefkow, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 202, p. 207 - 216
反应条件
1: NaBH4 2: PBr3 View Scheme
参考文献
Scherowsky, G.; Sefkow, M.
Molecular Crystals and Liquid Crystals (1969-1991), 1991 , vol. 202, p. 207 - 216
反应条件
1: 23 percent / silver hyponitrite / CH2Cl2 2: 92 percent / aq. KOH / methanol; tetrahydrofuran / 4 h / 0 - 20 °C View Scheme
参考文献
Ingold, K. U.; Paul, Thomas; Young, Mary Jane; Doiron, Leanne
Journal of the American Chemical Society, 1997 , vol. 119, # 50 p. 12364 - 12365
