P,P-二乙基膦酰基乙酸烯丙酯合成路线 （共 5 条）
反应条件
potassium carbonate; triphenylphosphine; sodium 2-ethyl hexanoate in DMF (N,N-dimethyl-formamide) T=30 - 40°C; 1 h;
参考文献
Korea Institute of Science and Technology
Patent: US2004/87633 A1, 2004 ;
Location in patent: Page 7 ;
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane T=20°C; Esterification; 18 h;
参考文献
Blades, Kevin; Butt, Afshan H.; Stuart Cockerill; Easterfield, Howard J.; Lequeux, Thierry P.; Percy, Jonathan M.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 24 p. 3609 - 3614
反应条件
potassium hydroxide 1.) EtOH, 25 deg C, 16 h; 2.) DMF, 25 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 111, # 20 p. 8036 - 8037
参考文献
Hoffmann, Reinhard W.; Ditrich, Klaus
Liebigs Annalen der Chemie, 1990 , # 1 p. 23 - 29
参考文献
Zhurnal Obshchei Khimii, , vol. 24, p. 1855,1859;engl.Ausg.S.1819,1821
