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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1132-27-0
合成路线
（共 13 条）
1132-27-0
+
10365-98-7
3-甲氧基苯硼酸
→
反应条件
4373-67-5
3-(3-甲氧基苯基)吡啶
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
905966-46-3
+
1132-27-0
→
反应条件
21308-81-6
3-(3-噻吩)吡啶
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 14 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
1132-27-0
+
44767-62-6
1-己基氯化镁
→
反应条件
6311-92-8
3-正-己基吡啶
反应条件
N,N'-di(2,4,6-trimethylphenyl)-4,5-dihydroimidazolinium chloride; iron(II) chloride in tetrahydrofuran; dichloromethane T=65°C; 3 h; Inert atmosphereSealed tube;
参考文献
Silberstein, Amanda L.; Ramgren, Stephen D.; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 14 p. 3796 - 3799
1132-27-0
+
693-04-9
氯丁基镁
→
反应条件
539-32-2
3-丁基吡啶
反应条件
FeF3*3H2O; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in tetrahydrofuran; diethyl ether 8 h; Inert atmosphereReflux; Reagent/catalyst;
参考文献
Agrawal, Toolika; Cook, Silas P.
Organic Letters, 2013 , vol. 15, # 1 p. 96 - 99
1132-27-0
+
1314538-55-0
[(叔丁氧羰基氨基)甲基]三氟硼酸钾
→
反应条件
102297-41-6
N-Boc-3-氨甲基吡啶
反应条件
C45H59ClNPPd; potassium carbonate in water; tert-butyl alcohol T=85°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 10 p. 2534 - 2537
1132-27-0
+
98-80-6
苯硼酸
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
1132-27-0
→
反应条件
1008-88-4
3-苯基吡啶
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
1132-27-0
+
99768-12-4
4-甲氧羰基苯硼酸
→
反应条件
90395-47-4
4-(3-吡啶)苯甲酸甲酯
反应条件
potassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki coupling; Inert atmosphere;
参考文献
Chen, Guo-Jun; Han, Fu-She
European Journal of Organic Chemistry, 2012 , # 19 p. 3575 - 3579
905966-40-7
+
1132-27-0
→
反应条件
90395-47-4
4-(3-吡啶)苯甲酸甲酯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
110-91-8
吗啉
+
1132-27-0
→
反应条件
92670-29-6
反应条件
[NiCl2(1,2-dimethoxyethane)]; 4,4,5,5-tetramethyl-2-phenyl-[1,3,2]-dioxaborolane; sodium t-butanolate; SIDip*HCl in 1,4-dioxane T=23 - 80°C; 4 h; Inert atmosphere;
参考文献
Hie, Liana; Ramgren, Stephen D.; Mesganaw, Tehetena; Garg, Neil K.
Organic Letters, 2012 , vol. 14, # 16 p. 4182 - 4185
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