NAlpha,NAlpha-二(羧基甲基)-L-赖氨酸水合物合成路线 (共 5 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 12 h;
参考文献
Lin, Yu-Chung; Liang, Ming-Ren; Lin, Yu-Chen; Chen, Chao-Tsen
Chemistry - A European Journal, 2011 , vol. 17, # 46 p. 13059 - 13067
反应条件
dimercaptoethane; tri-iso-propylsilane; phenol; trifluoroacetic acid T=20°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 29 p. 10205 - 10215
反应条件
1: NaOH / H2O / 0 - 50 °C 2: H2 / Pd-on-charcoal / methanol; H2O / 2 h / 20 °C / 760.05 Torr View Scheme
参考文献
Analytical Chemistry, , vol. 78, # 17 p. 6065 - 6073
反应条件
1: 94 percent / H2 / Pd/C / methanol / 6 h / 20 °C 2: phenol; triisopropylsilane; ethanedithiol / trifluoroacetic acid / H2O / 4 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 128, # 7 p. 2365 - 2372
反应条件
sodium hydrogencarbonate in diethyl ether; water
T=20°C; Cooling with ice;
参考文献
ATOMIC ENERGY COUNCIL - INSTITUTE OF NUCLEAR ENERGY RESEARCH; LIN, CHIH-YUAN; CHANG, YU; WANG, JEN-TSUNG; HSU, CHENG-FANG; KUO, WEI-TI; YU, HUNG-WEN; LIN, WUU-JYH; WANG, MEI-HUI
Patent: US2014/46045 A1, 2014 ;
Location in patent: Paragraph 0071 - 0074 ;