4-氟-5-硝基-1,2-苯二胺合成路线 （共 4 条）
反应条件
sulfuric acid T=85°C; 0.5 h;
参考文献
Nasielski-Hinkens, Raymonde; Leveque, Pierre; Castelet, Daniel; Nasielski, Jacques
Heterocycles, 1987 , vol. 26, # 9 p. 2433 - 2442
反应条件
1: 84 percent / 50percent aq. phosphinic acid / 10percent Pd/C / methanol / 0.33 h / Heating 2: 95 percent / pyridine / 18 h / 85 °C 3: 70 percent / fuming HNO3, CH3COOH / 0.67 h 4: 90 percent / aq. H2SO4 / 0.5 h / 85 °C View Scheme
参考文献
Heterocycles, , vol. 26, # 9 p. 2433 - 2442
反应条件
1: 95 percent / pyridine / 18 h / 85 °C 2: 70 percent / fuming HNO3, CH3COOH / 0.67 h 3: 90 percent / aq. H2SO4 / 0.5 h / 85 °C View Scheme
参考文献
Heterocycles, , vol. 26, # 9 p. 2433 - 2442
反应条件
1: 70 percent / fuming HNO3, CH3COOH / 0.67 h 2: 90 percent / aq. H2SO4 / 0.5 h / 85 °C View Scheme
参考文献
Heterocycles, , vol. 26, # 9 p. 2433 - 2442
