反应条件
1.1: (-)-Dibenzoyl-L-tartaric acid / isopropyl alcohol; water / 24 h / 20 °C
2.1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / |Cooling with ice
3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0.08 h / 0 °C
4.1: sodium hydroxide / dichloromethane / 0.5 h / 20 °C
4.2: 2 h / |Reflux
View Scheme
参考文献
Tsang, Althea S.-K.; Ingram, Katrin; Keiser, Jennifer; Hibbert, D. Brynn; Todd, Matthew H.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 30 p. 4921 - 4924