2-氨基-9,9-二己基芴合成路线 （共 4 条）
反应条件
palladium 10 on activated carbon; hydrazine hydrate in ethanol 2 h; Inert atmosphereReflux;
参考文献
Barik, Satyananda; Friedland, Sayuri; Skene
Canadian Journal of Chemistry, 2010 , vol. 88, # 9 p. 945 - 953
反应条件
1.1: phenylmethyltriethylammonium bromide; sodium hydroxide / water; dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere 1.2: 96 h / 20 °C / Inert atmosphere 2.1: nitric acid / 2 h / Inert atmosphere; Reflux 3.1: palladium 10 on activated carbon; hydrazine hydrate / ethanol / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Barik, Satyananda; Friedland, Sayuri; Skene
Canadian Journal of Chemistry, 2010 , vol. 88, # 9 p. 945 - 953
反应条件
1.1: phenylmethyltriethylammonium bromide; sodium hydroxide / water; dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere 1.2: 96 h / 20 °C / Inert atmosphere 2.1: nitric acid / 2 h / Inert atmosphere; Reflux 3.1: palladium 10 on activated carbon; hydrazine hydrate / ethanol / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Barik, Satyananda; Friedland, Sayuri; Skene
Canadian Journal of Chemistry, 2010 , vol. 88, # 9 p. 945 - 953
反应条件
1: nitric acid / 2 h / Inert atmosphere; Reflux 2: palladium 10 on activated carbon; hydrazine hydrate / ethanol / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Barik, Satyananda; Friedland, Sayuri; Skene
Canadian Journal of Chemistry, 2010 , vol. 88, # 9 p. 945 - 953
