4-甲基-N-丙基-苯磺酰胺合成路线 (共 6 条)
反应条件
triethylsilane; boron trifluoride diethyl etherate in benzene
T=5°C; 15 h;
参考文献
Alexander, Michael D.; Anderson, Robert E.; Sisko, Joseph; Weinreb, Steven M.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2563 - 2564
参考文献
Adamczyk, Maciej; Johnson, Donald D.; Mattingly, Phillip G.; Moore, Jeffrey A.; Pan, You
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 15 p. 3917 - 3921
反应条件
sodium hypochlorite; acetic acid
T=20°C; 16 h;
参考文献
Gibson, Susan E.; Kaufmann, Karina A. C.; Loch, Jennifer A.; Steed, Jonathan W.; White, Andrew J. P.
Chemistry - A European Journal, 2005 , vol. 11, # 8 p. 2566 - 2576
反应条件
titanium tetrachloride in tetrachloroethane, 1,1,2,2-
T=120°C; 48 h; sealed tube;
参考文献
Chen, Jiayan; Dang, Ling; Li, Qiang; Ye, Yong; Fu, Shaomin; Zeng, Wei
Synlett, 2012 , # 4 p. 595 - 600
反应条件
Duolite (A-101D (Cl(-) form)
1.) water, 2.) 5 h; Yield given. Multistep reaction;
参考文献
Sanghavi, N.M.; Parab, V.L.; Patravale, B. S.; Patel, M. N.
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1499 - 1504
反应条件
1-methoxy-2-phenylprop-1-enolate in tetrahydrofuran
T=-78°C; 1 h; other reagent; Product distribution;
参考文献
Differding, Edmond; Lang, Robert W.
Helvetica Chimica Acta, 1989 , vol. 72, p. 1248 - 1252