6-甲氧基-3,3-二甲基-1-茚满酮合成路线 （共 11 条）
参考文献
Horii et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 163,165, 166
Chem.Abstr., 1956 , p. 13850
反应条件
1: Br2, alkaline
2: 1.) PCl5, 2.) AlCl3 / 1) C6H6
3: KNO3, H2SO4 / 0 °C
4: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
5: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
1: KNO3, H2SO4 / 0 °C
2: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
3: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
1: 1.) PCl5, 2.) AlCl3 / 1) C6H6
2: KNO3, H2SO4 / 0 °C
3: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
4: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
1: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
2: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
1: AlCl3
2: Br2, alkaline
3: 1.) PCl5, 2.) AlCl3 / 1) C6H6
4: KNO3, H2SO4 / 0 °C
5: 1.) H2, 2.) NaNO2, HCl, 3.) H2SO4, H2O / 1.) PtO / 2) 0 deg C; 3) heating
6: K2CO3 / acetone
View Scheme
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
potassium carbonate in acetone
参考文献
Bott, Garry; Field, Leslie D.; Sternhell, Sever
Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5618 - 5626
反应条件
aluminium trichloride; benzene
参考文献
Horii et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 163,165, 166
Chem.Abstr., 1956 , p. 13850
Full Text Show Details
Goo-on et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 305,309
反应条件
1: (i) CuI, (ii) aq. HCl
2: aq. KOH
3: P2O5, H3PO4
View Scheme
参考文献
Kundu,A.K. et al.
Journal of the Chemical Society, 1965 , p. 2749 - 2763
反应条件
1: NH4OAc
2: (i) CuI, (ii) aq. HCl
3: aq. KOH
4: P2O5, H3PO4
View Scheme
参考文献
Kundu,A.K. et al.
Journal of the Chemical Society, 1965 , p. 2749 - 2763
