1-[2-(三甲基硅基)乙氧羰氧基]苯并三唑合成路线 (共 2 条)
反应条件
triethylamine in acetonitrile 1.) 0 deg C, 15 min; 2.) room temp., overnight; Yield given;
参考文献
Fan, Jinda; Brown, Sarah M.; Tu, Zhude; Kharasch, Evan D.
Bioconjugate Chemistry, 2011 , vol. 22, # 4 p. 752 - 758
反应条件
1: K2CO3 / toluene / 1.) -10 to -5 deg C, 30 min; 2.) room temp., 1 h 2: triethylamine / acetonitrile / 1.) 0 deg C, 15 min; 2.) room temp., overnight View Scheme
参考文献
Shute, Richard E.; Rich, Daniel H.
Synthesis, 1987 , # 4 p. 346 - 349