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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
113349-27-2
合成路线
（共 8 条）
113349-27-2
→
反应条件
458-35-5
松柏醇
反应条件
sodium phosphate-citrate buffer; β-glucosidase T=37°C; 24 h;
参考文献
Popravko, S. A.; Sokolov, I. V.; Torgov, I. V.
Chemistry of Natural Compounds, 1984 , vol. 20, # 2 p. 140 - 147
Khimiya Prirodnykh Soedinenii, 1984 , vol. 20, # 2 p. 152 - 160
113349-27-2
→
反应条件
458-35-5
松柏醇
反应条件
sodium phosphate-citrate buffer; β-glucosidase T=37°C; 24 h;
参考文献
Popravko, S. A.; Sokolov, I. V.; Torgov, I. V.
Chemistry of Natural Compounds, 1984 , vol. 20, # 2 p. 140 - 147
Khimiya Prirodnykh Soedinenii, 1984 , vol. 20, # 2 p. 152 - 160
864757-97-1
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1.1: n-buthyllithium / hexane; tetrahydrofuran / 0.17 h / -65 °C<br />1.2: triisopropyl borate / tetrahydrofuran / 0.17 h / -65 °C<br />1.3: hydrochloric acid / H<sub>2</sub>O<br />2.1: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />3.1: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
2595-07-5
烯丙基-beta-吡喃半乳糖苷
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: 100 percent / 4-N,N-dimethylaminopyridine; pyridine / 1 h / 20 °C<br />2: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />3: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
50-99-7
葡萄糖
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1: 68 percent / immobilized β-D-glucosidase / 72 h / 50 °C<br />2: 100 percent / 4-N,N-dimethylaminopyridine; pyridine / 1 h / 20 °C<br />3: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />4: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
7368-78-7
4-溴邻甲氧基苯酚
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 4 steps<br /> </b>1.1: 75 percent / hydrochloric acid / acetonitrile / 24 h / 20 °C<br />2.1: n-buthyllithium / hexane; tetrahydrofuran / 0.17 h / -65 °C<br />2.2: triisopropyl borate / tetrahydrofuran / 0.17 h / -65 °C<br />2.3: hydrochloric acid / H<sub>2</sub>O<br />3.1: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />4.1: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
10343-15-4
烯丙基-四-O-乙酰基-beta-D-吡喃葡萄糖苷
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />2: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
182344-21-4
(4-羟基-3-甲氧基苯基)硼酸
→
反应条件
113349-27-2
反应条件
<b>Multi-step reaction with 2 steps<br /> </b>1: 42 percent / copper(II) acetate; lithium acetate; palladium(II) acetate / dimethylformamide / 0.5 h / 80 °C<br />2: 99 percent / NaOMe / methanol / 1 h<br /> <br />
参考文献
Kishida, Masashi; Akita, Hiroyuki Tetrahedron, 2005 , vol. 61, # 44 p. 10559 - 10568
