3-(2-甲基氨基乙基)-1H-吲哚-5-醇合成路线 (共 5 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran; diethyl ether Heating;
参考文献
Heterocycles, , vol. 46, p. 91 - 94
反应条件
1: 76 percent / 8 percent aq. NaOH / methanol / 0.17 h / 60 °C 2: 65 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 26 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 49, # 1 p. 87 - 96
反应条件
1: 24 percent / H2O / 0.33 h / 20 °C 2: 65 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 26 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 49, # 1 p. 87 - 96
反应条件
1: 94 percent / pyridine / dimethylformamide / 1.5 h / 0 - 20 °C 2: 65 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 26 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 49, # 1 p. 87 - 96
反应条件
1: 60 percent / aq. HCl / methanol / 0.33 h / 0 - 20 °C 2: 65 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 26 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 49, # 1 p. 87 - 96