(R)-1-(2-呋喃)乙基醋酸盐合成路线 (共 14 条)
反应条件
Pseudomonas cepacia lipase in 1,1,1,2-tetrafluoroethane 24 h; Resolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Tetrahedron Letters, , vol. 50, # 26 p. 3543 - 3546
反应条件
hydrogen; P,P'-1,2-Phenylenebislt;(1R,2S,4R,5S)-2,5-dimethyl-7-phosphabicyclolt;2.2.1gt;heptanegt;; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in methanol P=1275.1 Torr; 24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 4 p. 516 - 518
反应条件
[Ru(CO)2Cl(C5Bn5)]; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=23°C; 9 h; Inert atmospheredynamic kinetic resolutionEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1452 - 1457
反应条件
Candida antarctica lipase B; (η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=20°C; 6 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 24 p. 8817 - 8825
参考文献
Journal of Organic Chemistry, , vol. 53, # 7 p. 1586 - 1587
反应条件
Candida antarctica lipase B in toluene T=23°C; 1.5 h; Resolution of racemate; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 9 p. 1317 - 1320
反应条件
in hexane 24 h; lipozyme-IM;
参考文献
Tetrahedron Asymmetry, , vol. 7, # 3 p. 907 - 910
反应条件
Pseudomonas cepacia lipase; 4 A molecular sieve; peracetylated-β-cyclodextrin in toluene T=40°C; 8 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 17 p. 2547 - 2555
反应条件
Pseudomonas fluorescence Amano AKG lipase in cyclohexane T=36°C; 2 h;
参考文献
Synthetic Communications, , vol. 37, # 13 p. 2163 - 2170
反应条件
Lipase PS Amano from Burkholderia cepacia in di-isopropyl ether T=25°C; 24 h; Resolution of racemateIonic liquidsolid phase reactionEnzymatic reaction; optical yield given as percent ee;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 67, # 1-2 p. 129 - 134