5-羟基-环己烷-1,3-二羧酸 二甲酯合成路线 (共 3 条)
反应条件
hydrogen; acetic acid; Rh/Al2O3 in methanol T=0 - 25°C; P=2844.39 Torr;
参考文献
US2011/98299 A1, ;
Page/Page column 40 ;
反应条件
1: triethylamine; pyridine-SO3 complex / dichloromethane; dimethyl sulfoxide / 10 - 25 °C / Inert atmosphere 2: diethylamino-sulfur trifluoride / dichloromethane; ethanol / 0 - 25 °C / Inert atmosphere View Scheme
参考文献
H. LUNDBECK A/S
Patent: US2011/98299 A1, 2011 ;
反应条件
pyridine-SO3 complex; triethylamine in dichloromethane; dimethyl sulfoxide
T=10 - 25°C; Inert atmosphere;
参考文献
H. LUNDBECK A/S
Patent: US2011/98299 A1, 2011 ;
Location in patent: Page/Page column 40 ;