2,4-二氰基-3-乙基-3-甲基戊二酰亚胺合成路线 （共 5 条）
反应条件
methanol; lithium nitride T=20°C; 12 h; sealed;
参考文献
Wu, Liqiang; Yang, Chunguang; Yang, Liming; Yang, Lijuan
Heterocycles, 2009 , vol. 78, # 4 p. 977 - 982
参考文献
Thole; Thorpe
Journal of the Chemical Society, 1911 , vol. 99, p. 440
Full Text Show Details
Thorpe; Wood
Journal of the Chemical Society, 1913 , vol. 103, p. 1575
Journal of the Chemical Society, 1923 , vol. 123, p. 63
反应条件
sulfuric acid; water
参考文献
Holder, Richard W.; Daub, John P.; Baker, Wesley E.; Gilbert, Raymond H; Graf, Norman A.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1445 - 1451
反应条件
80 percentige Schwefelsaeure;
参考文献
Thorpe; Wood
Journal of the Chemical Society, 1913 , vol. 103, p. 1575
Journal of the Chemical Society, 1923 , vol. 123, p. 63
反应条件
1: 95 percent / H2SO4, H2O
2: 91 percent / H2SO4 / toluene / 24 h / Heating
3: 84 percent / sodium / toluene / 28 h / Heating
4: 69 percent / 85 percent phosphoric acid / 85 h
View Scheme
参考文献
Holder, Richard W.; Daub, John P.; Baker, Wesley E.; Gilbert, Raymond H; Graf, Norman A.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1445 - 1451
