反应条件
Mg in diethyl ether
(N2); addn. of bromide deriv. to magnesium in ether, refluxing for 2 h, cooling to room temp., addn. of soln. of tin compd. in ether, refluxing for 4 h; addn. of aq. HCl, extn. (diethyl ether), drying over MgSO4, filtration, evapn., recrystn. (diethyl ether), elem. anal.;
参考文献
Miller, Philip W.; Nieuwenhuyzen, Mark; Charmant, Jonathan P. H.; James, Stuart L.
Inorganic Chemistry, 2008 , vol. 47, # 18 p. 8367 - 8379
