反应条件
HCl in diethyl ether addn. of 1,5-dibromopentane in dry ether to Mg turnings, slow addn. of diphenyl tin dichloride in dry ether (room temp.), refluxing (3 h), cooling, hydrolysis by pouring in ice-cold 1M HCl; decanting of organic layer, washing (10percent KF soln.), decanting, drying (MgSO4), removing of solvent, distn. of residual oil (395-398 K, 13 Pa); elem. anal.;
参考文献
Carson, A. S.; Jamea, E. H.; Laye, P. G.; Spencer, J. A.
Journal of Chemical Thermodynamics, 1988 , vol. 20, # 8 p. 923 - 926
