反应条件
1: 65 percent / Me3SiCN / acetonitrile / 39 h / 90 °C
2: DIBAH / toluene / 4.5 h / from -78 deg C to 20 deg C
3: 20percent aqu.sodium, potassium tartrate / 5 h / 20 °C
4: 10 percent / NaBH4 / ethanol / 0.5 h / -60 °C
View Scheme
参考文献
Berlage, Ulrich; Schmidt, Juergen; Milkova, Zenka; Welzel, Peter
Tetrahedron Letters, 1987 , vol. 28, # 27 p. 3095 - 3098
