4-戊烯-1-基2,3,4,6-四-O-苄基-D-吡喃葡萄糖苷合成路线 (共 16 条)
反应条件
sodium hydride in N,N-dimethyl-formamide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 2 p. 317 - 320
反应条件
1.1: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide; diisopropylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C / |Inert atmosphere 1.2: 24 h / 60 °C / |Inert atmosphere 2.1: [Btz-Au-PPh3]OTf / dichloromethane / 0.5 h / 20 °C / |Molecular sieve View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 39 p. 5231 - 5234
反应条件
N-bromosuccinmide; water in acetonitrile 2.33 h; Ambient temperature;
参考文献
Rodebaugh, Robert; Fraser-Reid, Bert
Tetrahedron, 1996 , vol. 52, # 22 p. 7663 - 7678
反应条件
N-bromosuccinmide 7 h; Ambient temperature; Further byproducts given;
参考文献
Ratcliffe, Andrew J.; Fraser-Reid, Bert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 747 - 750
反应条件
N-bromosuccinmide; water in acetonitrile 2.33 h; Ambient temperature;
参考文献
Rodebaugh, Robert; Fraser-Reid, Bert
Tetrahedron, 1996 , vol. 52, # 22 p. 7663 - 7678
反应条件
N-bromosuccinmide 7 h; Ambient temperature; Further byproducts given;
参考文献
Ratcliffe, Andrew J.; Fraser-Reid, Bert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 747 - 750