1: tetramethylguanidinium azide (TMGA) / CH2Cl2 / 9 h / 25 °C 2: 96 percent / lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 0 °C 3: 99 percent / H2 / 10percent Pd/C / H2O; acetic acid / 3 h / 760 Torr View Scheme
参考文献
Evans, David A.; Britton, Thomas C.; Ellman, Jonathan A.; Dorow, Roberta L.
Journal of the American Chemical Society, 1990 , vol. 112, # 10 p. 4011 - 4030
