1: methyl-magnesium iodide With trimethylsilyl-methylmagnesium chloride; lithium chloride; zinc(II) chloride in tetrahydrofuran; diethyl ether T=20°C; Grignard addition; 2: 1-thiophen-3-yl-ethanone in tetrahydrofuran; diethyl ether T=0°C; Grignard addition; 3 h;

暂无反应条件数据

caesium carbonate; 1-methyl-naphthalene; biphenyl-2-yl-di-tert-butyl-phosphane; palladium diacetate in toluene 8 h; Heating;

caesium carbonate; 1-methyl-naphthalene; biphenyl-2-yl-di-tert-butyl-phosphane; palladium diacetate in toluene 8 h; Heating;