反应条件
1: BH3 / tetrahydrofuran; methanol / Heating
2: 99 percent / 1N HCl / tetrahydrofuran / Ambient temperature
3: 88 percent / Et3N, trifluoracetic acid / dimethylsulfoxide; CH2Cl2 / -78 °C
4: p-TsOH / dioxane / Heating
5: 97 percent / NaBH4 / methanol / -78 deg C then room temp.
View Scheme
参考文献
Burkholder; Fuchs
Journal of the American Chemical Society, 1990 , vol. 112, # 26 p. 9601 - 9613