4-甲基-2-(甲硫基)嘧啶合成路线 （共 7 条）
反应条件
5 palladium on charcoal; camphor-10-sulfonic acid; hydrogen T=20 - 140°C; P=30003 Torr; 24 h; Autoclave;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; FONDS DE DEVELOPPEMENT DES FILIERES DES OLEAGINEUX ET PROTEAGINEUX FIDOP; Lemaire, Marc; Dayoub, Wissam; Sutter, Marc; Raoul, Yann
Patent: US2014/18579 A1, 2014 ;
Location in patent: Paragraph 0121 ;
反应条件
5 palladium on charcoal; camphor-10-sulfonic acid; hydrogen T=20 - 145°C; P=7500.75 Torr; 24 h; Autoclave;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; FONDS DE DEVELOPPEMENT DES FILIERES DES OLEAGINEUX ET PROTEAGINEUX FIDOP; Lemaire, Marc; Dayoub, Wissam; Sutter, Marc; Raoul, Yann
Patent: US2014/18579 A1, 2014 ;
Location in patent: Paragraph 0122 ;
反应条件
hydrogen; platinum(IV) oxide in ethanol
参考文献
Piantadosi,C. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2425 - 2428
反应条件
1: Na / diethyl ether 2: H2 / PtO2 / ethanol View Scheme
参考文献
Piantadosi,C. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2425 - 2428
参考文献
Eremenko,L.T.; Korolev,A.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, # 2 p. 399 - 401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, # 2 p. 440 - 444
反应条件
sodium hydride 1.) THF, room temperature, 2.) reflux; Multistep reaction;
参考文献
Doren, Henk A. van; Geest, Ralph van der; Kellogg, Richard M.; Wynberg, Hans
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 3 p. 197 - 203
反应条件
nitric acid; acetic anhydride
参考文献
Eremenko,L.T.; Korolev,A.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, # 2 p. 399 - 401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, # 2 p. 440 - 444
