4-甲氧基-联苯-4-胺合成路线 (共 16 条)
反应条件
potassium carbonate in ethanol T=78°C; Suzuki-Miyaura coupling; 1 h; Air atmosphere;
参考文献
Zhou, Bo; Li, Yi-Qun
E-Journal of Chemistry, 2011 , vol. 8, # 4 p. 1490 - 1497
反应条件
palladium diacetate; potassium carbonate in tetrahydrofuran; water Suzuki-Miyaura coupling; 8 h; Inert atmosphereReflux;
参考文献
Razler, Thomas M.; Hsiao, Yi; Qian, Feng; Fu, Ruiling; Khan, Rana Kashif; Doubleday, Wendel
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1381 - 1384
反应条件
tetrabutyl ammonium fluoride; potassium carbonate in water T=100°C; Suzuki-Miyaura coupling; 8 h;
参考文献
Yamada, Yoichi M. A.; Sarkar, Shaheen M.; Uozumi, Yasuhiro
Journal of the American Chemical Society, 2012 , vol. 134, # 6 p. 3190 - 3198
反应条件
Ru/C; potassium hydroxide in ethanol; toluene T=120°C; 12 h; Microwave irradiation;
参考文献
Kim, Ju Hyun; Park, Ji Hoon; Chung, Young Keun; Park, Kang Hyun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2412 - 2418
反应条件
nitric acid; acetic acid in methanol; water; N,N-dimethyl-formamide; toluene
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol T=60°C; 24 h; Microwave irradiation;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 13 p. 2412 - 2418
反应条件
palladium diacetate; potassium carbonate in tetrahydrofuran; water Suzuki-Miyaura coupling; 12 h; Inert atmosphereReflux;
参考文献
Journal of Organic Chemistry, , vol. 74, # 3 p. 1381 - 1384
反应条件
tetrabutylammomium bromide; potassium carbonate; quasi polymeric 4-pyridine-aldoxime Pd(II)-catalyst T=120°C; Suzuki-Miyaura reaction; 0.333333 h; microwave irradiation;
参考文献
Solodenko, Wladimir; Schoen, Uwe; Messinger, Josef; Glinschert, Anja; Kirschning, Andreas
Synlett, 2004 , # 10 p. 1699 - 1702
反应条件
1: palladium 10 on activated carbon; sodium carbonate / ethanol; water / 3 h / |Reflux 2: hydrogen / ethanol; water / 1.5 h / 20 °C / 760.05 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 35 p. 4772 - 4775
反应条件
1: palladium 10 on activated carbon; sodium carbonate / ethanol; water / 3 h / |Reflux 2: hydrogen / ethanol; water / 1.5 h / 20 °C / 760.05 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 35 p. 4772 - 4775