N,N-二甲基-4-联苯胺合成路线 （共 82 条）
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
C32H26ClN2NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=85°C; 12 h; Inert atmosphere;
参考文献
Zhang, Xue-Qi; Wang, Zhong-Xia
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3658 - 3663
反应条件
[NiCl2(PMe3)2] in tetrahydrofuran
T=70°C; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Zhong-Xia
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1641 - 1645
反应条件
trifluorormethanesulfonic acid
1.) 0 deg C, 1 h, 2.) room temperature, 4 h;
参考文献
Shudo, Koichi; Ohta, Toshiharu; Okamoto, Toshihiko
Journal of the American Chemical Society, 1981 , vol. 103, # 3 p. 645 - 653
反应条件
P[2,4,6-(OMe)3C6H2]3; bis(acetylacetonate)nickel(II) in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=25°C; 24 h;
参考文献
Manolikakes, Georg; Dastbaravardeh, Navid; Knochel, Paul
Synlett, 2007 , # 13 p. 2077 - 2080
反应条件
Ni(PCy3)2Cl2 in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=90°C; Negishi coupling reaction; 8 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Angewandte Chemie - International Edition, 2011 , vol. 50, # 21 p. 4901 - 4904
反应条件
triphenyl phosphite; K3PO4*3H2O; Ipr.HCl; palladium diacetate in tert-butyl alcohol
T=80°C; 10 h; Inert atmosphere;
参考文献
Chen, Xiaofeng; Ke, Haihua; Chen, Yao; Guan, Changwei; Zou, Gang
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7572 - 7578
反应条件
trifluorormethanesulfonic acid
Ambient temperature;
参考文献
Shudo, Koichi; Ohta, Toshiharu; Okamoto, Toshihiko
Journal of the American Chemical Society, 1981 , vol. 103, # 3 p. 645 - 653
反应条件
xanthone powder in acetonitrile
Irradiation;
参考文献
Milanesi, Silvia; Fagnoni, Maurizio; Albini, Angelo
Chemical Communications, 2003 , # 2 p. 216 - 217
反应条件
triethylamine in 2,2,2-trifluoroethanol
4 h; Photolysis;
参考文献
De Carolis, Marco; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 8 p. 1232 - 1236
