(顺式)-1,1'-(1,2-环丙烷二基)二苯合成路线 (共 66 条)
反应条件
hydrogen; palladium on activated charcoal in pentane
P=25857.4 Torr; 0.5 h; Ambient temperature;
参考文献
Matsui, Yasushi; Orchin, Milton
Journal of Organometallic Chemistry, 1983 , vol. 244, # 4 p. 369 - 374
反应条件
gold in 1,2-dichloro-ethane
T=20°C; 24 h; Inert atmosphere; optical yield given as percent de;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
gold in 1,2-dichloro-ethane
T=80°C; 24 h; Inert atmosphere; optical yield given as percent de;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
in dichloromethane
T=-78°C; Yield given;
参考文献
Brookhart, M.; Humphrey, M. B.; Kratzer, H. J.; Nelson, G. O.
Journal of the American Chemical Society, 1980 , vol. 102, # 26 p. 7802 - 7803
反应条件
iodine; diethylzinc in dichloromethane
T=20°C; Simmons-Smith Cyclopropanation; 2.5 h; Inert atmosphere; Overall yield = 71 percent; Overall yield = 69 mg; diastereoselective reaction;
参考文献
Levesque, Eric; Goudreau, Sebastien R.; Charette, Andre B.
Organic Letters, 2014 , vol. 16, # 5 p. 1490 - 1493
反应条件
potassium hydroxide in diethylene glycol
T=200 - 230°C; 0.75 h; Yield given. Yields of byproduct given;
参考文献
Applequist, Douglas E.; Gdanski, Rick D.
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2502 - 2510
反应条件
copper acetylacetonate in 1,2-dichloro-ethane
T=25°C;
参考文献
Berkessel, Albrecht; Kaiser, Patrick; Lex, Johann
Chemistry - A European Journal, 2003 , vol. 9, # 19 p. 4746 - 4756
反应条件
HMn(CO)5; carbon monoxide; sodium lauryl sulfate in water
T=50°C; 14 h; Yield given. Yields of byproduct given;
参考文献
Matsui, Yasushi; Orchin, Milton
Journal of Organometallic Chemistry, 1983 , vol. 244, # 4 p. 369 - 374
反应条件
n-butyllithium in tetrahydrofuran
T=-78°C; 0.7 h; Yields of byproduct given;
参考文献
Krief, Alain; Hobe, Myriam; Dumont, Willy; Badaoui, Elie; Guittet, Eric; Evrard, Guy
Tetrahedron Letters, 1992 , vol. 33, # 23 p. 3381 - 3384
反应条件
potassium carbonate in 1,4-dioxane
T=110°C; optical yield given as percent de;
参考文献
Barluenga, Jose; Quinones, Noelia; Tomas-Gamasa, Maria; Cabal, Maria-Paz
European Journal of Organic Chemistry, 2012 , # 12 p. 2312 - 2317