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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1138-62-1
合成路线
（共 10 条）
1138-62-1
+
5720-05-8
4-甲基苯硼酸
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in toluene T=180°C; Suzuki-Miyaura cross-coupling; 0.166667 h; Microwave irradiationInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 5 p. 1507 - 1510
905966-40-7
+
1138-62-1
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
1138-62-1
+
98-80-6
苯硼酸
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
1138-62-1
+
5123-13-7
5,5-二甲基-2-苯基-1,3,2-二氧硼杂
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
110-91-8
吗啉
+
1138-62-1
→
反应条件
27347-14-4
4-(4-甲氧基苯基)吗啉
反应条件
[Ni0(1,5-cyclooctadiene)2]; sodium t-butanolate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 1,4-dioxane T=80°C; 3 h; Inert atmosphere;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; GARG, Neil K.; RAMGREN, Stephen D.; SILBERSTEIN, Amanda L.; QUASDORF, Kyle W.
Patent: WO2012/94622 A2, 2012 ;
Location in patent: Page/Page column 22-23; 24 ;
1138-62-1
+
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
1138-62-1
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
morpholine; C31H45Cl2N3OPd; caesium carbonate in water T=110°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
参考文献
Wang, Zhan-Yong; Ma, Qin-Na; Li, Ren-Hao; Shao, Li-Xiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7899 - 7906
1138-62-1
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
1138-62-1
+
693-04-9
氯丁基镁
→
反应条件
18272-84-9
4-丁基苯甲醚
反应条件
FeF3*3H2O; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in tetrahydrofuran; diethyl ether 8 h; Inert atmosphereReflux; Reagent/catalyst;
参考文献
Agrawal, Toolika; Cook, Silas P.
Organic Letters, 2013 , vol. 15, # 1 p. 96 - 99
1138-62-1
+
335343-05-0
→
反应条件
49602-47-3
2,4-二甲氧基联苯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 60 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
