trimethylsilyl trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C; 16 h;
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N.
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
Multi-step reaction with 3 steps 1: 78 percent / triphenylphosphine/carbon tetrabromide / dimethylformamide / 16 h / 20 °C2: 100 percent / 4 h / Heating3: sulfuric acid / acetic acid / 18 h / 20 °C
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N. Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
Multi-step reaction with 5 steps 1: 85 percent / triethylamine / dioxane / 1 h / 20 °C2: 89 percent / tin tetrachloride / 1,2-dichloro-ethane / 0.08 h / 20 °C3: 78 percent / triphenylphosphine/carbon tetrabromide / dimethylformamide / 16 h / 20 °C4: 100 percent / 4 h / Heating5: sulfuric acid / acetic acid / 18 h / 20 °C
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N. Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
Multi-step reaction with 4 steps 1: 89 percent / tin tetrachloride / 1,2-dichloro-ethane / 0.08 h / 20 °C2: 78 percent / triphenylphosphine/carbon tetrabromide / dimethylformamide / 16 h / 20 °C3: 100 percent / 4 h / Heating4: sulfuric acid / acetic acid / 18 h / 20 °C
参考文献
Mikhailov, Sergei N.; Padyukova, Nelly Sh.; Karpeiskii, Marat Ya.; Kolobushkina, Lidiya I.; Beigelman, Leon N. Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 4 p. 1055 - 1066
