三(乙腈)五甲基环戊二烯基三氟甲磺酸钌(II)合成路线 (共 3 条)
反应条件
Ag(OSO2CF3) in acetonitrile Refluxing, 2 h, AgOTf added.; Filtd., evapd., ether added.;
参考文献
Fagan, Paul J.; Ward, Michael D.; Caspar, Jonathan V.; Calabrese, Joseph C.; Krusic, Paul J.
Journal of the American Chemical Society, 1988 , vol. 110, p. 2981 - 2983
反应条件
in acetonitrile byproducts: AgCl; refluxing for 1 h, cooling to room temp.; filtn., washing (diethyl ether), drying in vac., elem. anal.;
参考文献
Fagan, Paul J.; Ward, Michael D.; Calabrese, Joseph C.
Journal of the American Chemical Society, 1989 , vol. 111, # 5 p. 1698 - 1719
反应条件
trifluoromethanesulfonic acid potassium salt; zinc T=20°C; 2 h;
参考文献
Degussa AG
Patent: EP1394170 A1, 2004 ;
Location in patent: Page/Page column 10 ;