Gerrard,W. et al.
Journal of the Chemical Society, 1962 , p. 113 - 119
Full Text View citing articles Show Details
Gmelin Handbook: B: B-Verb.4, 4.4.2, page 118 - 120
hydrogenchloride in tetrahydrofuran; benzene
(Ar); to THF soln. of Grignard reagent was added boron compd. in benzene and react. quenched after 15 min with aq. HCl, soln. was extd. with ether, dried (Na2SO4) exts. evapd. in vac. and residual oil treated with ethanolamine; after 5 min mixt. was poured into ether/water (1:1), pptd. product was filtered off and recrystd. from EtOH;
参考文献
Lapin, Stephen C.; Brauer, Beth-Ellen; Schuster, Gary B.
Journal of the American Chemical Society, 1984 , vol. 106, # 7 p. 2092 - 2100
