反应条件
Multi-step reaction with 4 steps 1.1: 87 percent / K2CO3 / dimethylsulfoxide / 2 h / 100 °C2.1: LiClO4; MeONa / methanol / Electrochemical reaction2.2: H2O / 0.75 h / 55 °C3.1: LDA / tetrahydrofuran / 1.5 h / -80 - -15 °C3.2: 72 percent / tetrahydrofuran / 0 °C4.1: 72 percent / NaBH4 / ethanol / 0 °C
参考文献
Girard, Nicolas; Pouchain, Laurent; Hurvois, Jean-Pierre; Moinet, Claude Synlett, 2006 , # 11 p. 1679 - 1682
