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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1139705-29-5
合成路线
（共 7 条）
273-53-0
苯并恶唑
+
1139705-29-5
→
反应条件
14625-56-0
反应条件
palladium diacetate; caesium carbonate; 1,2-bis-(diphenylphosphino)ethane in 1-methyl-pyrrolidin-2-one T=100°C; 14 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Barfuesser, Sebastian; Pospech, Jola
Organic Letters, 2010 , vol. 12, # 4 p. 724 - 726
67-56-1
甲醇
+
201230-82-2
+
1139705-29-5
→
反应条件
2459-25-8
2-萘甲酸甲酯
反应条件
(BINAP)PdCl2; triethylamine T=50 - 55°C; P=3345.86 Torr;
参考文献
Albaneze-Walker, Jennifer; Raju, Ravinder; Vance, Jennifer A.; Goodman, Andrew J.; Reeder, Michael R.; Liao, Jing; Maust, Mathew T.; Irish, Patrick A.; Espino, Peter; Andrews, David R.
Organic Letters, 2009 , vol. 11, # 7 p. 1463 - 1466
1139705-29-5
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
+
321903-29-1
1,3-二氢-1,1-二甲基-2,1-苯并氧硅杂环戊二烯
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium carbonate in dimethyl sulfoxide T=110°C; Hiyama coupling;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
1139705-29-5
+
536-74-3
苯乙炔
→
反应条件
23975-17-9
反应条件
potassium phosphate; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in dimethyl sulfoxide T=65°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
1139705-29-5
+
67-64-1
丙酮
→
反应条件
21567-68-0
反应条件
palladium diacetate; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=80°C; 8 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Mehta, Vaibhav P.
Chemistry - A European Journal, 2012 , vol. 18, # 33 p. 10230 - 10233
1139705-29-5
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
+
321903-29-1
1,3-二氢-1,1-二甲基-2,1-苯并氧硅杂环戊二烯
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium carbonate in dimethyl sulfoxide T=110°C; Hiyama coupling;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
1139705-29-5
+
5720-05-8
4-甲基苯硼酸
→
反应条件
59115-49-0
(6CI,7CI)-2-对甲苯萘
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate in N,N-dimethyl acetamide; water T=60°C; Suzuki-Miyaura cross-coupling;
参考文献
Albaneze-Walker, Jennifer; Raju, Ravinder; Vance, Jennifer A.; Goodman, Andrew J.; Reeder, Michael R.; Liao, Jing; Maust, Mathew T.; Irish, Patrick A.; Espino, Peter; Andrews, David R.
Organic Letters, 2009 , vol. 11, # 7 p. 1463 - 1466
