1-乙酰基-2-苯基肼合成路线 （共 133 条）
反应条件
sodium hydride in tetrahydrofuran
T=20°C; 18 h;
参考文献
Hisler, Kevin; Commeureuc, Aurelien G.J.; Zhou, Sheng-ze; Murphy, John A.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3290 - 3293
反应条件
sodium hydroxide in benzene
参考文献
Barinova, V. N.; Voronin, V. G.; Zhestkov, V. P.; Portnov, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1609 - 1611
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1765 - 1767
反应条件
1: 15 percent / 40percent aq. NaOH / benzene
2: 80 percent / 40percent aq. NaOH / benzene / 6 h / 20 - 25 °C
View Scheme
参考文献
Barinova, V. N.; Voronin, V. G.; Zhestkov, V. P.; Portnov, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1609 - 1611
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1765 - 1767
参考文献
Atkinson; Polya
Journal of the Chemical Society, 1952 , p. 3418,3421,3422
反应条件
1: diethyl ether; petroleum ether
2: alcohol; sulfuric acid
3: sodium nitrite; aqueous-alcoholic hydrochloric acid
View Scheme
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1924 , vol. 43, p. 853
反应条件
1: 32 percent / diisopropylethylamine / toluene / 48 h / 80 °C
2: 95 percent / 6N HCl / 2 h / Heating
View Scheme
参考文献
Bhatia, Pramila A.; Brooks, Clint D. W.; Basha, Anwer; Ratajczyk, James D.; Gunn, Bruce P.; Bouska, Jennifer B.; Lanni, Carmine; Young, Patrick R.; Bell, Randy L.; Carter, George W.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 20 p. 3938 - 3950
反应条件
T=0 - 50°C; Inert atmosphere;
参考文献
O'Toole, Sarah E.; Connon, Stephen J.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 17 p. 3584 - 3593
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid in 1,2-dichloro-ethane
T=70°C; 16 h; Inert atmosphere;
参考文献
Zhao, Dongbing; Shi, Zhuangzhi; Glorius, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12426 - 12429
Angew. Chem., 2013 , vol. 125, # 47 p. 12652 - 12656,4
反应条件
phosphorus trichoride
参考文献
Michaelis; Schenk
Chemische Berichte, 1908 , vol. 41, p. 3872
反应条件
phosphorus trichoride
参考文献
Michaelis; Schenk
Chemische Berichte, 1907 , vol. 40, p. 3569
