1-乙酰基-2-苯基肼合成路线 （共 133 条）
参考文献
Michaelis; Schenk
Chemische Berichte, 1907 , vol. 40, p. 3569
反应条件
1: diethyl ether / 100 °C / im geschlossenen Rohr
View Scheme
参考文献
Pellizzari
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 39
参考文献
Grammaticakis
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1938 , vol. 207, p. 239
反应条件
lithium aluminium tetrahydride
参考文献
Kratzl; Berger
Monatshefte fuer Chemie, 1958 , vol. 89, p. 83,84, 86
反应条件
ethanol; anhydrous copper acetate
参考文献
Gattermann; Johnson; Hoelzle
Chemische Berichte, 1892 , vol. 25, p. 1080
反应条件
1.1: sodium / ethanol / 20 h / 100 °C / |Sealed tube; |Darkness
2.1: copper(l) iodide; potassium carbonate; N,N-dimethylethylenediamine / toluene / 24 h / 110 °C / |Schlenk technique; |Inert atmosphere
2.2: 1 h / 90 °C
View Scheme
参考文献
Zhan, Fuxu; Liang, Guangxin
Angewandte Chemie - International Edition, 2013 , vol. 52, # 4 p. 1266 - 1269
Angew. Chem., 2012 , vol. 125, # 4 p. 1304 - 1307,4
反应条件
1: sodium amide / 220 °C
2: piperidine; benzene
View Scheme
参考文献
Stanek; Rybar
Chemicke Listy, 1946 , vol. 40, p. 173,176
Chem.Abstr., 1951 , p. 5147
反应条件
sodium hydroxide in benzene
参考文献
Barinova, V. N.; Voronin, V. G.; Zhestkov, V. P.; Portnov, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1609 - 1611
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 8 p. 1765 - 1767
反应条件
1: LiAlH4
2: LiAlH4
View Scheme
参考文献
Kratzl; Berger
Monatshefte fuer Chemie, 1958 , vol. 89, p. 83,84, 86
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; caesium acetate; acetic acid in 1,2-dichloro-ethane
T=100°C; 16 h; Inert atmosphere;
参考文献
Zhao, Dongbing; Shi, Zhuangzhi; Glorius, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12426 - 12429
Angew. Chem., 2013 , vol. 125, # 47 p. 12652 - 12656,4
