叔丁基2-氧代氮杂丁烷-1-羧酸合成路线 （共 4 条）
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=0 - 20°C; Inert atmosphere;
参考文献
Prasad, Gitanjeli; Amoroso, Jon W.; Borketey, Lawrence S.; Schnarr, Nathan A.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 10 p. 1992 - 2002
反应条件
Schwartz's reagent in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Piperno, Anna; Carnovale, Caterina; Giofr, Salvatore V.; Iannazzo, Daniela
Tetrahedron Letters, 2011 , vol. 52, # 51 p. 6880 - 6882
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen in tert-butyl alcohol T=80°C; P=22502.3 Torr; 24 h; Autoclave;
参考文献
Ito, Masato; Koo, Lee Wei; Himizu, Akio; Kobayashi, Chika; Sakaguchi, Ayaka; Ikariya, Takao
Angewandte Chemie - International Edition, 2009 , vol. 48, # 7 p. 1324 - 1327
反应条件
1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere 2: dirhodium tetraacetate / toluene / 110 °C / Inert atmosphere View Scheme
参考文献
Hovey, M. Todd; Eklund, Emily J.; Pike, Robert D.; Mainkar, Anshul A.; Scheerer, Jonathan R.
Organic Letters, 2011 , vol. 13, # 5 p. 1246 - 1249
