2-(4-氯苯基)-苯并噁唑合成路线 (共 59 条)
反应条件
iodine; N,N-dimethyl-formamide in chlorobenzene
T=130°C;
参考文献
Teo, Yew Chin; Riduan, Siti Nurhanna; Zhang, Yugen
Green Chemistry, 2013 , vol. 15, # 9 p. 2365 - 2368
反应条件
1: DBU / PdCl2(PPh3)2, PPh3 / N,N-dimethyl-acetamide / 0.5 h / 120 °C / 4654.3 Torr
2: conc. HCl / N,N-dimethyl-acetamide / 16 h / Heating
View Scheme
参考文献
Perry, Robert J.; Wilson, B. David; Miller, Richard J.
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2883 - 2887
反应条件
copper(l) iodide; oxygen; palladium diacetate; potassium carbonate in 1,4-dioxane
T=120°C; 48 h; Sealed tube;
参考文献
Zhang, Manli; Zhang, Shouhui; Liu, Miaochang; Cheng, Jiang
Chemical Communications, 2011 , vol. 47, # 41 p. 11522 - 11524
反应条件
[RuCl(CO)(PPh3)(PNS-Me)]; potassium hydroxide in toluene
T=100°C; 24 h;
参考文献
Ramachandran, Rangasamy; Prakash, Govindan; Selvamurugan, Sellappan; Viswanathamurthi, Periasamy; Malecki, Jan Grzegorz; Ramkumar, Venkatachalam
Dalton Transactions, 2014 , vol. 43, # 21 p. 7889 - 7902
反应条件
palladium diacetate; copper (II) acetate monohydrate; potassium carbonate; triphenylphosphine in toluene
3 h; Refluxunder air;
参考文献
Yan, Xue-Ming; Mao, Xue-Rong; Huang, Zhi-Zhen
Heterocycles, 2011 , vol. 83, # 6 p. 1371 - 1376
反应条件
PPA
T=100 - 120°C; Addition; 12 h;
参考文献
So, Ying-Hung; DeCaire, Richard
Synthetic Communications, 1998 , vol. 28, # 22 p. 4123 - 4135
反应条件
in cyclohexane
24 h; Irradiation;
参考文献
Taylor, Edward C.; Katz, Alan H.; Alvarado, Sergio I.; McKillop, Alexander
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1607 - 1609
反应条件
1: methanol / Heating
2: iodobenzene diacetate / methanol
View Scheme
参考文献
Prakash, Om; Batra, Anita; Sharma, Vijay; Saini, Rajesh K.; Verma, Rajender S.
Journal of the Indian Chemical Society, 2003 , vol. 80, # 11 p. 1031 - 1034
反应条件
in ethanol
Ambient temperature;
参考文献
Abdelhamid, Abdou O.; Parkanyi, Cyril; Rashid, S. M. Khaledur; Lloyd, Winston D.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 403 - 405
反应条件
1: 99 percent / tetrahydrofuran / 24 h / 20 °C
2: 99 percent / CuI; Cs2CO3; 1,10-phenanthroline / 1,2-dimethoxy-ethane / 24 h / Heating
View Scheme
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808